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Deoxygenation of Nitrosobenzene by the Electrogenerated Pd3(dppm)3(μ3-CO) Cluster

✍ Scribed by Cyril Cugnet; David Brevet; Sophie Dal Molin; Dominique Lucas; Yves Mugnier; Pierre D. Harvey

Book ID: 106406353
Publisher: Springer
Year: 2007
Tongue: English
Weight: 357 KB
Volume: 18
Category: Article
ISSN: 1040-7278
DOI: 10.1007/s10876-007-0135-8

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## Abstract Addition of formate on the dicationic cluster [Pd~3~(dppm)~3~(μ~3~‐CO)]^2+^ (dppm=bis(diphenylphosphinomethane) affords quantitatively the hydride cluster [Pd~3~(dppm)~3~(μ~3~‐CO)(μ~3~‐H)]^+^. This new palladium–hydride cluster has been characterised by ^1^H NMR, ^31^P NMR and UV/Vis sp

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Comparison in halide binding ability between the unsaturated clusters [Pd3(μ-dppm)3(CO)]2+ and [PdPtCo(μ-dppm)2(CO)3(CNtBu)]+ (dppm = Ph2PCH2PPh2)

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