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Darstellung von P(III)- und P(III/V)-Oxyden

โœ Scribed by Prof. Dr. E. Thilo; Dr. D. Heinz; Dr. K.-H. Jost

Publisher
John Wiley and Sons
Year
1964
Tongue
English
Weight
228 KB
Volume
76
Category
Article
ISSN
0044-8249

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PhCN#iMe3)3 (1) reacts with PhPCI2 in a molar ratio of 2: 3 to give the bicyclic system 2 with a P(V)-P(III)-P(V) unit, characterized by an X-ray structure analysis. Dichlorophenylphosphane reacts with [MetNC(NH&JCI (3) to form 4. The reaction of MeNCN with LiN(SiMe& and PhPCI2 yields 5 containing a