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Cycloadditions XX. Crystal and molecular structure of the adduct from 3-diazobutanone and carbon disulfide

✍ Scribed by Kapecki, Jon A.; Baldwin, John E.; Paul, Iain C.

Book ID: 127280885
Publisher: American Chemical Society
Year: 1968
Tongue: English
Weight: 657 KB
Volume: 90
Category: Article
ISSN: 0002-7863
DOI: 10.1021/ja01023a025

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The structure of the adduct from 3-diazo

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✍ Jon A. Kapecki; John E. Baldwin; Iain C. Paul 📂 Article 📅 1967 🏛 Elsevier Science 🌐 French ⚖ 156 KB

Printed in great Britain\* (Received in USA 21 AuLugust 1967) 3-Diazo?Jutaaoneinrefluxing carbon disulfide afforda anadduct C&&$\*ldBichm beem assigned stnxture Ia (or its gemetric iraner) (2), a fomulation analogous to Ib

The structure of the adduct from 3-diazo

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N-[Benzyl]isoquinolinium halides and carbon disulfide heated in strongly basic aqueous dioxane give adducts which have been assigued structure I (2). The available evidence (2) is equally consistent with the alternative formulation II. For an analogous base-catalyzed reaction between an N-[benayll-5

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