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Crystal Structure of the Bis(Picrato-O,O")Tetraaquacalcium Complex with 18-Crown-6, [Ca(Pic)2(H2O)4] · 18C6

✍ Scribed by A. N. Chekhlov

Book ID
110314262
Publisher
SP MAIK Nauka/Interperiodica
Year
2001
Tongue
English
Weight
70 KB
Volume
27
Category
Article
ISSN
1070-3284

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## Abstract Reaction of TiF~4~ and 18‐crown‐6 in MeCN affords the molecular complex [(__cis‐__TiF~4~)~2~(18‐crown‐6)] (1) only. Water and THF displace the 18‐crown‐6 in the tetrafluoro complex 1, with the formation of __cis‐__TiF~4~L~2~. The complex __cis‐__TiF~4~(H~2~O)~2~ and 18‐crown‐6 form [{__