𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Crystal structure of lactitol (4-O-β-d-galactopyranosyl-d-glucitol) trihydrate

✍ Scribed by Jussi Kivikoski; Ilkka Pitkänen; Juha Nurmi


Publisher
Elsevier Science
Year
1992
Tongue
English
Weight
408 KB
Volume
232
Category
Article
ISSN
0008-6215

No coin nor oath required. For personal study only.

✦ Synopsis


Lactitol trihydrate, C12H24O11.3H2O, crystallises in the orthorhombic space group, P2(1)2(1)2(1) with cell dimensions a = 8.306(2), b = 10.163(1), c = 21.321(1) A, and V = 1799.8(5) A3; Z = 4, Dx = 1.47 Mg m-3, lambda(Cu-K alpha) = 1.54178 A, mu = 1.14 mm-1, F(000) = 856, and T = 23 degrees. There are one intra- and thirteen inter-molecular hydrogen bonds in the structure. The bond lengths and angles agree well with the mean values of related structures. The galactopyranosyl ring has a chair conformation.


📜 SIMILAR VOLUMES


Crystal structure of lactitol (4-O-β-d-g
✍ Jussi Kivikoski; Ilkka Pitkänen; Jussi Valkonen; Heikki Heikkilä 📂 Article 📅 1992 🏛 Elsevier Science 🌐 English ⚖ 410 KB

Lactitol, C12H24O11, is monoclinic, space group P2(1) with cell dimensions a = 7.614(1), b = 10.757(1), c = 9.370(1) A, beta = 108.19(1) degrees, and V = 729.0(1) A3, Z = 2, Dx = 1.57 Mg.m-3, lambda (Cu-K alpha) = 1.54056 A, mu = 1.166 mm-1, F(000) = 368, and T = 23 degrees. The structure was solved

Crystal structure of lactitol (4-O-β-d-g
✍ Jussi Kivikoski; Jussi Valkonen; Juha Nurmi 📂 Article 📅 1992 🏛 Elsevier Science 🌐 English ⚖ 429 KB

Lactitol dihydrate, C12H24O11.2H2O, is tetragonal, space group P4(3)2(1)2 with cell dimensions a and b = 8.7612(1), c = 45.500(3) A, and V = 3493.2(3) A3, Z = 8, Dx = 1.45 Mg.m-3, lambda (Cu-K alpha) = 1.54056 A, mu = 1.108 mm-1, F(000) = 1632, and T = 23 degrees. The structure was solved by direct

Synthesis and characterization of propyl
✍ Hamdy A. El-Shenawy; Conrad Schuerch 📂 Article 📅 1984 🏛 Elsevier Science 🌐 English ⚖ 571 KB

Ally1 4-0-(4-O-acetyl-2-O-benzoyl-3,6-di-O-benzyl-~-D-galactopyranosyl)-2-0-benzoyl-3,6-di-O-benzyl-a-D-galactopyranoside was 0-deallylated to give the 1-hydroxy derivative, and this was converted into the corresponding l-O-(Nphenylcarbamoyl) derivative, treatment of which with dry HCl produced the

The crystal structure of diazomethyl β-d
✍ J.Robert Paddison Jr.; Tuli P. Haromy; Muttaiya Sundaralingam; Robert W. Myers; 📂 Article 📅 1987 🏛 Elsevier Science 🌐 English ⚖ 415 KB

The title compound (C8H12N2O6) crystallizes in the orthorhombic space group P2(1)2(1)2(1) (Z = 4), with a = 4.871(1), b = 11.136(2), c = 18.301(2) A. The structure was solved by the multi-solution technique and refined by full-matrix least-squares to a final R-index of 0.042. The compound adopts the