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The crystal structure of diazomethyl β-d-galactopyranosyl ketone

✍ Scribed by J.Robert Paddison Jr.; Tuli P. Haromy; Muttaiya Sundaralingam; Robert W. Myers; James N. beMiller

Publisher
Elsevier Science
Year
1987
Tongue
English
Weight
415 KB
Volume
168
Category
Article
ISSN
0008-6215

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✦ Synopsis

The title compound (C8H12N2O6) crystallizes in the orthorhombic space group P2(1)2(1)2(1) (Z = 4), with a = 4.871(1), b = 11.136(2), c = 18.301(2) A. The structure was solved by the multi-solution technique and refined by full-matrix least-squares to a final R-index of 0.042. The compound adopts the 4C1(D) conformation. Bond lengths in the diazoacetyl group are consistent with the presence of a zwitterion.

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