Crystal and molecular structure of complex cis-[(VAL)2Pd]·H20
✍ Scribed by V. Z. Pletnev; Yu. A. Zolotarev; N. M. Galitskii; A. I. Verenich
- Publisher
- SP MAIK Nauka/Interperiodica
- Year
- 1992
- Tongue
- English
- Weight
- 313 KB
- Volume
- 33
- Category
- Article
- ISSN
- 0022-4766
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Synthesis, Crystal Structure, and Thermal Properties of cis-Pd(NH 3 ) 2 Br 2 . -The title complex is obtained by substitution of the oxalate group in [Pd(NH 3 ) 2 (C 2 O 4 )] by bromine. This electro-neutral planar complex possesses a molecular-type crystal structure (space group Pbca, Z=8) and has
## Abstract The peptide N‐Ac‐dehydro‐Phe‐L‐Val‐L‐Val‐OCH~3~ (C~22~H~31~N~3~O~5~) was synthesized by the usual workup procedure and finally by coupling the N‐Ac‐dehydro‐Phe‐L‐Val‐OH to valine methyl ester. It was crystallized from its solution in acetonitrile‐water mixture at 4°C. The crystals belon