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Crystal and Molecular Structure of cis-Trioxatris-σ-homobenzene (cis-“Benzene Trioxide”)

✍ Scribed by Dr. Walter Littke; Dipl.-Chem. Ulrich Drück

Publisher
John Wiley and Sons
Year
1974
Tongue
English
Weight
224 KB
Volume
13
Category
Article
ISSN
0044-8249

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trimethyl phosphite (in THF) to form benzene is fast at 20°C; nevertheless, neither the disulfide nor the monosulfide can be identified as intermediates ('H-NMR) under a variety of conditions (e.g. equimolar ratio; 20 "C). Apparently, elimination of the first sulfur atom has the highest activation e