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Coulometric and polarographic determinations of trace amounts of lead

✍ Scribed by Thomas L. Marple; L.B. Rogers


Publisher
Elsevier Science
Year
1954
Tongue
English
Weight
849 KB
Volume
11
Category
Article
ISSN
0003-2670

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Determination of oxygen in lead dioxide
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A sample of lead dioxide is reduced in the solid state in sodium hydroxide solution under conditions at which secondary reactions are negligible, so that the quantity of electricity passed is directly a measure of the reduced oxide. The inflexion observed in the cathode-potential-time plot is taken