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Convenient synthesis of d- and l-xylo-1,2,3,4-alkane tetrols from a d-gluco-configured common building block

✍ Scribed by Santosh Ramdas Borkar; Beedimane Narayana Manjunath; Sivaraman Balasubramaniam; Indrapal Singh Aidhen

Book ID: 116342903
Publisher: Elsevier Science
Year: 2012
Tongue: English
Weight: 460 KB
Volume: 358
Category: Article
ISSN: 0008-6215
DOI: 10.1016/j.carres.2012.06.005

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## Abstract Bis‐1,2,3,4‐tetrahydropyrimidinylalkanes/benzenes **2a‐f** have been synthesized by the reaction of N,S‐acetals with formaldehyde and diamines. Reaction of pyrazoles **3a** and **3b** with diamines and formaldehyde yield bis‐4,5,6,7‐tetrahydropyrazolo[3,4‐__d__]pyrimidinylalkanes **4a‐b