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Convenient One‐Pot Preparation of Dimethyl Bicyclo[2.2.2]octane‐1,4‐dicarbolylate, a Key Intermediate for a Novel Adenosine A 1 Receptor Antagonist

✍ Scribed by Chang, HeXi; Kiesman, William F.; Petter, Russell C.

Book ID
121358285
Publisher
Taylor and Francis Group
Year
2007
Tongue
English
Weight
110 KB
Volume
37
Category
Article
ISSN
0039-7911

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Efficient Large-Scale Synthesis of 4-Phenyl-3-butyn-2-one, a Key Intermediate for a Novel Potent Adenosine Antagonist. -A practical and facile large-scale synthesis of the 4-phenyl-3-butyn-2-one (IIIa) is presented based on the reaction of the in situ formed acetylenic Grignard reagent with two equ