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Convenient one-pot synthesis of benzoquinone-[U-14c] and hydroquinone-[U-14c]

✍ Scribed by Howard Parnes; Steve Dekeczer

Publisher
John Wiley and Sons
Year
1986
Tongue
French
Weight
338 KB
Volume
23
Category
Article
ISSN
0022-2135

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✦ Synopsis

Benzoquinone-[U-14C] was synthesized in 90% yield from benzene-[U-14C] via a three step oequence. Conditions were developed which allowed this conversion to be accomplished in a one pot closed system.

The b e n ~o q u i n o n e -[ U -~~C ] thus obtained could be reduced to h y d r o q u i n ~n e -[ U -~~C ]

in quantitative yield. Preparation of ben~ene-[U-~4C] is also described.

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