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CONVENIENT LARGE SCALE PREPARATION OF 5-METHYL- AND 4-NITRO- 2-IODOSOBENZOIC AND OF 4-NITRO-2-IODOXYBENZOIC ACIDS

✍ Scribed by Katritzky, Alan R.; Savage, G. Paul; Gallos, John K.; Durst, H. Dupont


Book ID
126904806
Publisher
Taylor and Francis Group
Year
1989
Tongue
English
Weight
339 KB
Volume
21
Category
Article
ISSN
0030-4948

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A simple four-stage conversion of 2-1nethyl-4(5>nitroimidazole to 2-methyl-4(5)-nitr0['~N""]imidazole is reported. The method consists in N-nitration of the initial compound to ?-methyl-1,4-dinitroimidazole, treating the latter with ["Nlglycine and N-dealkylation of the obtained (~-rnethyl-4-nitro[~