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The preparation of 3-methyl-4-nitro-5-(2-alkylethenyl)isoxazoles

โœ Scribed by Wells, Robert; Moccia, Maria; Adamo, Mauro F.A.

Book ID
121416031
Publisher
Elsevier Science
Year
2014
Tongue
French
Weight
285 KB
Volume
55
Category
Article
ISSN
0040-4039

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A simple four-stage conversion of 2-1nethyl-4(5>nitroimidazole to 2-methyl-4(5)-nitr0['~N""]imidazole is reported. The method consists in N-nitration of the initial compound to ?-methyl-1,4-dinitroimidazole, treating the latter with ["Nlglycine and N-dealkylation of the obtained (~-rnethyl-4-nitro[~