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Continuous Reactor Technology for Ketal Formation: An Improved Synthesis of Solketal

✍ Scribed by Clarkson, Jay S.; Walker, Andrew J.; Wood, Michael A.

Book ID
120212351
Publisher
American Chemical Society
Year
2001
Tongue
English
Weight
332 KB
Volume
5
Category
Article
ISSN
1083-6160

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## Abstract magnified image A library of 1,4‐disubstituted 1,2,3‐triazoles was synthesized using a copper flow reactor. Organic azides, generated __in situ__ from alkyl halides and sodium azide, were reacted with acetylenes using the copper‐catalyzed Huisgen 1,3‐dipolar cycloaddition. This process