Conformational study of two substance P hexapeptides by two-dimensional NMR
β Scribed by WONG, TUCK C. ;LEE, CHI MING ;GUO, WEI ;CHANG, DING-KWO
- Book ID
- 115099443
- Publisher
- Wiley (Blackwell Publishing)
- Year
- 2009
- Tongue
- English
- Weight
- 823 KB
- Volume
- 41
- Category
- Article
- ISSN
- 0367-8377
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π SIMILAR VOLUMES
## Abstract The ^1^H and ^13^C NMR spectra of eledoisin, an antidiuretic hormone, were studied by twoβdimensional NMR techniques. All the ^1^H and ^13^C NMR resonances were unambiguously determined from a combination of the 2D homoβ and heteroβnuclear NMR spectra.
## Combined utilization of 'H-IH homonuclear and 'H-l'C heteronuclear N M R chemical shift correlations, two-dimensional J-resolved 'H NMR measurements and homonuclear 'H double resonance experiments allowed specific assignments for both 'H and -C NMR frequencies to be made for the tricyclic sesqu