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Concerted use of homo- and hetero-nuclear 2D NMR: 13C and 1H assignment of sucrose octaacetate

✍ Scribed by Toshiaki Nishida; Curt R. Enzell; Gareth A. Morris

Publisher
John Wiley and Sons
Year
1986
Tongue
English
Weight
422 KB
Volume
24
Category
Article
ISSN
0749-1581

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✦ Synopsis

The complete assignment of the sugar and acetate 13C and 'H signals of sucrose octaacetate by homo-and hetero-nuclear 2D NMR is described, using the Jeenet (COSY) and relayed coherence transfer techniques and heteronuclear shift correlation via both one-bond and long-range couplings.

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