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Complete 1H and 13C assignments of ractopamine hydrochloride using 2D and selective 1D NMR methods

✍ Scribed by J. K. Huwe; S. Castellino; D. J. Smith

Publisher: John Wiley and Sons
Year: 1993
Tongue: English
Weight: 295 KB
Volume: 31
Category: Article
ISSN: 0749-1581
DOI: 10.1002/mrc.1260310314

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✦ Synopsis

Abstract

The ^1^H and ^13^C NMR resonances for ractopamine hydrochloride have been assigned. H,H‐COSY and H,C‐COSY were used to assign the aliphatic moiety of the molecule and to correlate protons and carbons on the same ring system. Long‐range selective proton decoupling (LSPD) experiments were used to assign quaternary carbons and to distinguish the two ring systems.

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