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Complete NMR analysis of oxytocin in phosphate buffer

✍ Scribed by Akiko Ohno; Nana Kawasaki; Kiyoshi Fukuhara; Haruhiro Okuda; Teruhide Yamaguchi

Publisher
John Wiley and Sons
Year
2009
Tongue
English
Weight
408 KB
Volume
48
Category
Article
ISSN
0749-1581

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✦ Synopsis

Abstract

Complete NMR analysis of oxytocin (OXT) in phosphate buffer was elucidated by one‐dimensional (1D)‐ and two‐dimensional (2D)‐NMR techniques, which involve the assignment of peptide amide NH protons and carbamoyl NH~2~ protons. The ^1^Hο£Ώ^15^N correlation of seven amide NH protons and three carbamoyl NH~2~ protons were also shown by HSQC NMR of OXT without ^15^N enrichment. Copyright Β© 2009 John Wiley & Sons, Ltd.

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