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Complete Assignments of the 13C NMR Spectra of Bilirubin-IXα and its Dimethyl Ester

✍ Scribed by Norbert Müller

Publisher
John Wiley and Sons
Year
1985
Tongue
English
Weight
322 KB
Volume
23
Category
Article
ISSN
0749-1581

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✦ Synopsis

Using two-dimensional heteronuclear 'H-13C chemical shift correlation spectroscopy via one-bond and long-range couplings, all 13C resonances of bilirubinl X a and its dimethyl ester in dimethyl sulphoxide solution are assigned, independently from reference to partial structures. Previous ambiguities in the methyl regions of the 'H NMR spectra of these compounds are also resolved. A / ,

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