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Complete assignments of the 1H and 13C NMR spectra of 15 limonoids

✍ Scribed by Benjamín Rodríguez

Publisher
John Wiley and Sons
Year
2003
Tongue
English
Weight
139 KB
Volume
41
Category
Article
ISSN
0749-1581

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✦ Synopsis

Abstract

Unambiguous and complete assignments of ^1^H and ^13^C NMR chemical shifts for 15 limonoids, eight of them found in natural sources and seven other synthetic derivatives, are presented. The assignments are based on 2D shift‐correlated [^1^H,^1^H‐COSY, ^1^H,^13^C‐gHSQC‐^1^J(C,H), ^1^H,^13^C‐gHMBC‐^n^J(C,H) (n = 2 and 3)] and NOE experiments. Copyright © 2003 John Wiley & Sons, Ltd.

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