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Complete assignments of 1H and 13C NMR spectral data of nine surfactin isomers

✍ Scribed by Jin-Shan Tang; Hao Gao; Kui Hong; Yang Yu; Miao-Miao Jiang; Hai-Peng Lin; Wen-Cai Ye; Xin-Sheng Yao

Publisher
John Wiley and Sons
Year
2007
Tongue
English
Weight
120 KB
Volume
45
Category
Article
ISSN
0749-1581

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✦ Synopsis

Abstract

A new surfactin isomer (1) was isolated from a mangrove bacteria strain ‘Bacillus sp’. Its structure was identified, and full assignments of ^1^H and ^13^C NMR spectral data were achieved for the first time by a combination of mass spectrometry and 1D and 2D NMR experiments including DEPT, ^1^H^1^H COSY, HSQC, HMBC, TOCSY, ROESY, and HSQC‐TOCSY. The NMR spectral data of eight known analogs (2–9) are also reported. Copyright © 2007 John Wiley & Sons, Ltd.

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