𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Complete assignments of 1H and 13C NMR spectral data for benzylidenebenzyl butyrolactone lignans

✍ Scribed by Rosangela da Silva; Susimaire Pedersoli; Valdemar Lacerda Junior; Paulo Marcos Donate; Sérgio de Albuquerque; Jairo Kenupp Bastos; Ana Lúcia Santos de Matos Araújo; Márcio Luis Andrade e Silva

Publisher
John Wiley and Sons
Year
2005
Tongue
English
Weight
94 KB
Volume
43
Category
Article
ISSN
0749-1581

No coin nor oath required. For personal study only.

✦ Synopsis

Abstract

The structures of three benzylidenebenzyl butyrolactone lignans (gossypifan, carthamogenin, and savinin) have been established on basis of ^1^H NMR and ^13^C NMR spectroscopic data. The ^1^H NMR and ^13^C NMR spectra of these lignans have been fully assigned by the use of techniques such as gCOSY, non‐edited gHSQC, and gHMBC. Complete assignment and most homonuclear hydrogen coupling constant measurements were performed, also providing enough data for the determination of the relative stereochemistry. Copyright © 2005 John Wiley & Sons, Ltd.

📜 SIMILAR VOLUMES

Complete assignments of 1H and 13C NMR s
Complete assignments of 1H and 13C NMR spectral data for arylnaphthalene lignan lactones
✍ Rosangela da Silva; Marcelo Maia Ruas; Paulo Marcos Donate 📂 Article 📅 2007 🏛 John Wiley and Sons 🌐 English ⚖ 90 KB 👁 1 views

## Abstract In this work we describe the complete ^1^H and ^13^C NMR analyses of three arylnaphtalene lignan lactones (taiwanin C, 4‐methyl dehydroretrodendrin and justicidin B) using modern NMR techniques such as gCOSY, nonedited gHSQC, gHMBC and NOE experiments. Complete assignment and homonuclea

Complete assignments of 1H and 13C NMR s
Complete assignments of 1H and 13C NMR spectral data for 7,7′-dihydroarylnaphthalene lignan lactones
✍ Rosangela da Silva; João Henrique Carvalho Batista; Carine da Silva Maringolo; P 📂 Article 📅 2009 🏛 John Wiley and Sons 🌐 English ⚖ 90 KB

## Abstract In this article we present a complete ^1^H and ^13^C NMR spectral analysis of three 7,7′‐dihydroarylnaphthalene lignan lactones using modern NMR techniques such as COSY, HSQC, HMBC and NOE experiments. Complete assignment and homonuclear hydrogen coupling constant measurements were perf

Complete assignment of 1H and 13C NMR da
Complete assignment of 1H and 13C NMR data for three aryltetralin lignan lactones
✍ Rosangela da Silva; Vladimir Constantino Gomes Heleno; Sérgio de Albuquerque; Ja 📂 Article 📅 2004 🏛 John Wiley and Sons 🌐 English ⚖ 97 KB 👁 1 views

## Abstract We describe the complete ^1^H and ^13^C NMR analysis of three aryltetralin lignan lactones (polygamain, morelensin and 4,5‐dimethoxymorelensin) using modern NMR techniques such as COSY, HMQC, HMBC, 2D‐__J__‐resolved and NOE experiments. The relative stereochemistry of these compounds, w

Complete assignments 1H and 13C NMR spec
Complete assignments 1H and 13C NMR spectral data of four anabaseine derivatives
✍ Eduardo Sobarzo-Sánchez; Julio De la Fuente; Elías Quezada; Luis Castedo 📂 Article 📅 2006 🏛 John Wiley and Sons 🌐 English ⚖ 103 KB 👁 1 views

## Abstract The anabaseine derivatives 6‐methoxy‐7‐hydroxy‐1‐(pyridin‐3‐yl)‐3,4‐dihydroisoquinoline, 6,7‐dimethoxy‐1‐(pyridin‐3‐yl)‐1,2,3,4‐tetrahydroisoquinoline and 6,7‐dimethoxy‐1‐(piperidin‐3‐yl)‐1,2,3,4‐tetrahydroisoquino‐ line were prepared either by demethylation with HBr or by reduction wit

Complete assignments of 1H and 13C NMR d
Complete assignments of 1H and 13C NMR data for seven arylnaphthalide lignans from Justicia procumbens
✍ Meihua Yang; Jun Wu; Fan Cheng; Yuan Zhou 📂 Article 📅 2006 🏛 John Wiley and Sons 🌐 English ⚖ 109 KB 👁 1 views

## Abstract Three new arylnaphthalide lignans named 6′‐hydroxy justicidin A (1), 6′‐hydroxy justicidin B (2) and 6′‐hydroxy justicidin C (3) have been isolated from the whole plant of __Justicia procumbens__, together with four known ones, neojusticin A (4), chinensinaphthol methyl ester (5), isodi

Complete assignments of 1H and 13C NMR d
Complete assignments of 1H and 13C NMR data for new dibenzocyclooctadiene lignans from Kadsura oblongifolia
✍ Hai-Tao Liu; Li-Jia Xu; Yong Peng; Jun-Shan Yang; Xiu-Wei Yang; Pei-Gen Xiao 📂 Article 📅 2009 🏛 John Wiley and Sons 🌐 English ⚖ 105 KB

## Abstract Two new dibenzocyclooctadiene lignans, named kadoblongifolins A (1) and B (2), and one new natural product dibenzocyclooctadiene lignan, named kadoblongifolin C (3), were isolated from the stems of __Kadsura oblongifolia__ (__K. oblongifolia__), together with five known ones, schizanrin