## Abstract A new surfactin isomer (1) was isolated from a mangrove bacteria strain ‘__Bacillus__ sp’. Its structure was identified, and full assignments of ^1^H and ^13^C NMR spectral data were achieved for the first time by a combination of mass spectrometry and 1D and 2D NMR experiments includin
Complete 1H and 13C NMR assignments and Z/E-stereoconfiguration determination of isomers of 1,4-diketone derivatives
✍ Scribed by Guohua Xu; Guodong Yin; Wenbo Guo; Anxin Wu; Yanfang Cui
- Publisher
- John Wiley and Sons
- Year
- 2007
- Tongue
- English
- Weight
- 137 KB
- Volume
- 46
- Category
- Article
- ISSN
- 0749-1581
- DOI
- 10.1002/mrc.2103
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✦ Synopsis
Abstract
Complete ^1^H and ^13^C NMR assignments and Z/E‐stereoconfiguration determination for a series of new isomers of 1,4‐diketone derivatives obtained via self‐sorting tandem reaction were accomplished by means of one‐ and two‐dimentional NMR experiments including ^1^H, ^13^C, gCOSY, gHSQC, gHMBC, and NOESY. Copyright © 2008 John Wiley & Sons, Ltd.
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