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Colorimetric analysis of immunogenic impurities in acetylsalicylic acid

โœ Scribed by Bundgaard, Hans


Book ID
121326504
Publisher
Pharmaceutical Press
Year
1976
Tongue
English
Weight
315 KB
Volume
28
Category
Article
ISSN
2042-7158

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Analysis of acetylsalicylic acid and ace
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methanol or acetone-ethanol gave rods, in. p. 85-86". Shoppee (5) gives m. p. 88-89" for p-sitosteryl chloride. Anal.-Calcd. for CggH4sC1; C1, 8.18. Found: C1, 8.15. p-Sitosterol 3,5Dinitrobenzoate.-The free compound (0.26 Gm.) was refluxed 0.5 hour with 0.60 Gm. 3,5-dinitrobenzoyl chloride in 8 m