Analysis of acetylsalicylic acid and ace
โ
Joseph Levine
๐
Article
๐
1961
๐
John Wiley and Sons
๐
English
โ 409 KB
methanol or acetone-ethanol gave rods, in. p. 85-86". Shoppee (5) gives m. p. 88-89" for p-sitosteryl chloride. Anal.-Calcd. for CggH4sC1; C1, 8.18. Found: C1, 8.15. p-Sitosterol 3,5Dinitrobenzoate.-The free compound (0.26 Gm.) was refluxed 0.5 hour with 0.60 Gm. 3,5-dinitrobenzoyl chloride in 8 m