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Chloro­[tris(p-methoxy­phenyl)­phosphine]­gold(I)

✍ Scribed by Ho, Soo Yei ;Tiekink, Edward R. T.

Publisher
International Union of Crystallography
Year
2001
Tongue
English
Weight
167 KB
Volume
57
Category
Article
ISSN
1600-5368

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Single-crystal X-ray study T = 223 K Mean '(C±C) = 0.005 A Ê R factor = 0.033 wR factor = 0.078 Data-to-parameter ratio = 25.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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The title compound, trans-[RhCl(C 18 F 15 P) 2 (CO)], crystallizes with one independent molecule in the asymmetric unit. Important geometric parameters are Rh-P = 2.2797 ( 14) and 2.2993 (14) A ˚, Rh-Cl = 2.3642 (12) A ˚, Rh-C = 1.824 (4) A ˚, C-Rh-Cl = 174.12 (13) , P-Rh-C = 91.73 (13) and 93.71 (1