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Chemistry of transition metal carbene complexes: nucleophilic substitution reactions of cyanamide anion to Fischer carbene complexes

✍ Scribed by Gangopadhyay, Sumana ;Mistri, Tarun ;Dolai, Malay ;Alam, Rabiul ;Ali, Mahammad

Book ID
118033141
Publisher
Royal Society of Chemistry
Year
2013
Tongue
English
Weight
894 KB
Volume
42
Category
Article
ISSN
1477-9226

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10 ml, and chromatographed on a silica gel column (Merck 0.05 to 0.2 mm; column dimensions 40 x 2 cm) at 0Β°C with hexane/benzene (4 : 1). The yellow zone is collected, the solvent removed in a high vacuum, and the residue recrystallized twice from n-pentane : pale yellow needles, m. p. 45 "C ; yield