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Atropisomerism of Transition Metal Carbene Complexes

✍ Scribed by Prof. Dr. Henri Brunner; Prof. Dr. Ernst Otto Fischer; Dipl.-Chem. Manfred Lappus

Publisher
John Wiley and Sons
Year
1971
Tongue
English
Weight
201 KB
Volume
10
Category
Article
ISSN
0044-8249

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✦ Synopsis

10 ml, and chromatographed on a silica gel column (Merck 0.05 to 0.2 mm; column dimensions 40 x 2 cm) at 0Β°C with hexane/benzene (4 : 1). The yellow zone is collected, the solvent removed in a high vacuum, and the residue recrystallized twice from n-pentane : pale yellow needles, m. p. 45 "C ; yield 250 mg (4%).

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