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Aldol reactions of transition metal carbene complexes

✍ Scribed by Wulff, William D.; Gilbertson, Scott R.


Book ID
120826553
Publisher
American Chemical Society
Year
1985
Tongue
English
Weight
369 KB
Volume
107
Category
Article
ISSN
0002-7863

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10 ml, and chromatographed on a silica gel column (Merck 0.05 to 0.2 mm; column dimensions 40 x 2 cm) at 0Β°C with hexane/benzene (4 : 1). The yellow zone is collected, the solvent removed in a high vacuum, and the residue recrystallized twice from n-pentane : pale yellow needles, m. p. 45 "C ; yield