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ChemInform Abstract: Total Synthesis of Milbemycin E: Development of a Procedure for the Introduction of the 3,4-Double Bond and Synthesis of the C(1)-C(10) Fragment.

โœ Scribed by E. R. PARMEE; S. V. MORTLOCK; N. A. STACEY; E. J. THOMAS; O. S. MILLS

Publisher
John Wiley and Sons
Year
2010
Weight
34 KB
Volume
28
Category
Article
ISSN
0931-7597

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ChemInform Abstract: Total Synthesis of
ChemInform Abstract: Total Synthesis of Milbemycin E: Resolution of the C(1)-C(10) Fragment and Final Assembly.
โœ P. G. STEEL; O. S. MILLS; E. R. PARMEE; E. J. THOMAS ๐Ÿ“‚ Article ๐Ÿ“… 2010 ๐Ÿ› John Wiley and Sons โš– 31 KB ๐Ÿ‘ 1 views

Total Synthesis of Milbemycin E: Resolution of the C(1)-C(10) Fragment and Final Assembly. -Resolution of the cyclohexanone (I) is the starting process in the preparation of title compound (VI). Key step is the coupling of butenolide (II) with phosphonium salt (III) (both prepared in the preceding p