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A Total Synthesis of Milbemycin G (II): Approaches to the C(1)—C(10)-Fragment (I) and Completion of the Synthesis.

✍ Scribed by Simon Bailey; Madeleine Helliwell; Aphiwat Teerawutgulrag; Eric J. Thomas

Publisher
John Wiley and Sons
Year
2006
Weight
13 KB
Volume
37
Category
Article
ISSN
0931-7597

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ChemInform Abstract: Total Synthesis of
ChemInform Abstract: Total Synthesis of Milbemycin E: Resolution of the C(1)-C(10) Fragment and Final Assembly.
✍ P. G. STEEL; O. S. MILLS; E. R. PARMEE; E. J. THOMAS 📂 Article 📅 2010 🏛 John Wiley and Sons ⚖ 31 KB 👁 2 views

Total Synthesis of Milbemycin E: Resolution of the C(1)-C(10) Fragment and Final Assembly. -Resolution of the cyclohexanone (I) is the starting process in the preparation of title compound (VI). Key step is the coupling of butenolide (II) with phosphonium salt (III) (both prepared in the preceding p