ChemInform Abstract: Theoretical Prediction of the Fundamental Properties for the Ternary Li 2 PtH 6 and Na 2 PtH 6
β Scribed by Ghebouli, M. A.; Choutri, H.; Bouarissa, N.; Ghebouli, B.; Bouhemadou, A.; Soyalp, F.; Ucgun, E.; Ocak, H. Y.
- Book ID
- 118756807
- Publisher
- John Wiley and Sons
- Year
- 2013
- Weight
- 18 KB
- Volume
- 44
- Category
- Article
- ISSN
- 0931-7597
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## Abstract The title compound is synthesized from mixtures of LiH and Pt in the presence of BH~3~NH~3~ (multiβanvil device, <8 GPa, 450β500 Β°C, 60 min) and characterized by powder XRD and IR spectroscopy.
## Abstract Key steps of the title synthesis are the previously developed pyrrole acylation method with monoethyl succinate (II) and the Suzuki cross coupling reaction of 3βchloroβ6βpyrrolylpyridazine (V) with arylboronic acids.
## Abstract A previously developed pyrrole acylation process using carboxylic acids and TFAA is successfully applied as the initial step in the synthesis of the starting material (VII).