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ChemInform Abstract: The Total Synthesis of Spirotryprostatin A.

✍ Scribed by S. D. EDMONDSON; S. J. DANISHEFSKY

Publisher: John Wiley and Sons
Year: 2010
Weight: 39 KB
Volume: 29
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.199831233

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✦ Synopsis

The Total Synthesis of Spirotryprostatin A.

-Key step in the synthesis of the title alkaloid (XI) which is found in the fermentation broth of Aspergillus fumigatus and which manifests cell cycle inhibition at the G2/M phase, is the rearrangement of a bromohydrin prepared in situ from β-carboline derivative (VI) using NBS. -(EDMONDSON,

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