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ChemInform Abstract: The Invention of Radical Reactions. Part 35. A Novel Radical Fission Reaction of N-Sulfonylthioxocarbamates.

✍ Scribed by D. H. R. BARTON; G. FONTANA; Y. YANG

Book ID: 112033270
Publisher: John Wiley and Sons
Year: 2010
Weight: 29 KB
Volume: 27
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.199625077

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Irradiation with visible light of N-hydraxy-2-thiopyridone esters f in the presence of sulphur dioxidrgave the corresponding th~os~fp~o~otes 4 in good yiefd. These could be converted to s&phones 5 by-treatment with KOH and an alkylating ogent. Alternatively, exposure to sulphuryl chloride followed b