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ChemInform Abstract: Synthesis of Enantiomerically Pure Constrained γ-Hydroxy-α- amino Acids by Directed Hydroxylation.

✍ Scribed by A. AVENOZA; C. CATIVIELA; M. PARIS; J. M. PEREGRINA; B. SAENZ-TORRE

Publisher
John Wiley and Sons
Year
2010
Weight
33 KB
Volume
28
Category
Article
ISSN
0931-7597

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✍ B. MERLA; H.-J. GRUMBACH; N. RISCH 📂 Article 📅 2010 🏛 John Wiley and Sons ⚖ 36 KB

Efficient Synthesis of γ-Oxo-and γ-Hydroxy-α-amino Acids. -Reduction of aminoester (Va) with Zn(BH 4 ) 2 permits intermediate isolation of the γ-hydroxy derivative, which is converted to lactone (IX) during silica gel chromatography. -(MERLA, B.;