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ChemInform Abstract: Synthesis of 2- and 6-Fluoro Analogues of threo-3-(3,4-Dihydroxyphenyl) serine (2- and 6-Fluoro-threo-DOPS).

โœ Scribed by B.-H. CHEN; J. NIE; M. SINGH; V. W. PIKE; K. L. KIRK

Book ID
112029970
Publisher
John Wiley and Sons
Year
2010
Weight
30 KB
Volume
27
Category
Article
ISSN
0931-7597

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A convenient synthesis of 2-fluoro- and 6-fluoro-(2S,3R)-threo-(3,4-dihydroxyphenyl)serine using Sharpless asymmetric aminohydroxylation
โœ In Ho Kim; Kenneth L Kirk ๐Ÿ“‚ Article ๐Ÿ“… 2001 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 58 KB

Ring-fluorinated b-hydroxy a-amino methyl esters 3b,c were synthesized enantioselectively using Sharpless asymmetric aminohydroxylation. These were converted to 2-fluoro-and 6-fluoro-(2S,3R)-threo-(3,4-dihydroxyphenyl)serine 1b,c using our previously published procedure.