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ChemInform Abstract: Synthesis and Structure of [Sn4Se11]6-, ∞1[Sn2Se52-], and ∞1[Sn3Se72-] — Model Anions for the Solventothermal Reaction Pathway to Lamellar Selenidostannates(IV).

✍ Scribed by Anja Loose; William S. Sheldrick

Publisher
John Wiley and Sons
Year
2010
Weight
37 KB
Volume
30
Category
Article
ISSN
0931-7597

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Synthesis and Structure of [Sn4Se11]6–,
Synthesis and Structure of [Sn4Se11]6–, 3.0.CO;2-M/asset/equation/tex2gif-stack-1.gif?v=1&t=h5l55r5t&s=b439cdb160594bc76a5be3d9bf20c7c44cb6e3bd" class="inlineGraphic"> [Sn2Se52–], and 3.0.CO;2-M/asset/equation/tex2gif-stack-2.gif?v=1&t=h5l55r5t&s=155c1d4a988fd3c89485d09b17a5955efa65189b" class="inlineGraphic"> [Sn3Se72–] – Model Anions for the Solventothermal Reaction Pathway to Lamellar Selenidostannates(IV)
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Reaction of A 2 CO 3 (A = K, Rb) with Sn and Se in an H 2 O/CH 3 OH mixture at 115±130 °C affords the isotypic selenidostannates(IV) A 6 Sn 4 Se 11 ´x H 2 O (A = K, x = 8) 1 and 2 whose discrete [Sn 4 Se 11 ] 6± anions each contain two corner-bridged ditetrahedral [Sn 2 Se 6 ] 4± species. Similar re

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ChemInform Abstract: The First Example of the Tetraselenidostannate Anion [SnSe4]4- as a Chelating Ligand to a Lanthanide Complex Ion: Solvothermal Synthesis and Characterization of Lanthanoid Selenidostannates [Hdien][Ln(dien)2(μ-SnSe4)] (Ln: Sm, Eu) and [Eu2(dien)4(μ-OH)2] Sn2Se6.
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