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ChemInform Abstract: Synthesis and Properties of 6-Oxo-3,5-dicyano-1,4,5,6-tetrahydrospiro( 4′-R-cyclohexane-1′,4-pyridine)-2-thiols and -selenols.

✍ Scribed by V. D. DYACHENKO; A. E. MITROSHIN; V. P. LITVINOV

Publisher
John Wiley and Sons
Year
2010
Weight
33 KB
Volume
28
Category
Article
ISSN
0931-7597

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✍ V. D. DYACHENKO; A. A. NIKISHIN; V. P. LITVINOV 📂 Article 📅 2010 🏛 John Wiley and Sons ⚖ 30 KB 👁 1 views

Ethylcrotonates in the Synthesis of 4,4-Disubstituted 3,5-Dicyano-6oxo-1,4,5,6-tetrahydropyridine-2-thiolates. -Michael addition of ethyl crotonate (I) to cyanothioacetamide (II) in the presence of N-methylmorpholine and subsequent in situ cyclization affords the title tetrahydropyridinethiolates as