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ChemInform Abstract: Synthesis and Magnetic Properties of LnFe10Si2Zx (Z: N, H and Ln: Tb, Er).

✍ Scribed by Q. M. CHENG; J. H. LIN; M. Z. SU

Publisher: John Wiley and Sons
Year: 2010
Weight: 35 KB
Volume: 29
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.199834019

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✦ Synopsis

Synthesis and Magnetic Properties of LnFe 10 Si 2 Zx (Z: N, H and Ln: Tb, Er).

-Single-phase products of LnFe 10 Si 2 are synthesized by a reduction-diffusion process from iron, silicon and Er 2 O 3 or Tb 4 O 7 together with excess calcium hydride (1. 950 • C, 2 h, 2. 1100 • C, 2.5 h). The nitrogen interstitial compounds are obtained by direct reaction with nitrogen at high pressure. The introduction of nitrogen changes the easy magnetization direction from the basal plane to the c-axis for TbFe 10 Si 2 and from the c-axis to the basal plane for ErFe 10

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