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ChemInform Abstract: Studies Directed Toward the Total Synthesis of Scytophycin C: Synthesis of the C1—C18 Fragment of Scytophycin C.

✍ Scribed by P. A. GRIECO; J. D. SPEAKE

Publisher
John Wiley and Sons
Year
2010
Weight
35 KB
Volume
29
Category
Article
ISSN
0931-7597

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✦ Synopsis

Studies Directed Toward the Total Synthesis of Scytophycin C: Synthesis of the C 1 -C 18 Fragment of Scytophycin C. -The synthesis of the C-1 to C-18 fragment (X) is based on a highly stereoselective carbon Ferrier-type rearrangement reaction of deoxyglucal (I) and the silyl enol ether (II). -(GRIECO, P. A.;

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The Total Synthesis of Scytophycin C. Part 1. Stereocontrolled Synthesis of the C 1 -C 32 Protected Seco Acid. -A stereocontrolled preparation of the C 1 -C 32 -seco acid ester (XI) required for the total synthesis of the macrolide scytophycin C is presented starting from the aldehyde (S)-(II) in 1