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ChemInform Abstract: Selective Syntheses of Bis[1,2]dithiolo[1,4]thiazines and Bis[1,2]dithiolopyrroles from Huenig′s Base.

✍ Scribed by C. W. REES; A. J. P. WHITE; D. J. WILLIAMS; O. A. RAKITIN; C. F. MARCOS; C. POLO; T. TORROBA

Publisher: John Wiley and Sons
Year: 2010
Weight: 35 KB
Volume: 29
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.199831117

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Selective Synthesis of Bis[1,2]dithiolo[

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ChemInform Abstract: Bis[1,2]dithiolo[3,4-b][4′,3′-e][1,4]thiazine-3,5-dione, a Planar 1,4-Thiazine.

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Bis [1,2]dithiolo [3,4-b][4',3'-e][1,4]thiazine-3,5-dione, a Planar 1,4-Thiazine. -Reaction of N-benzyldiisopropylamine (I) with S 2 Cl 2 gives N-benzyl-bisthiolothiazine (II) with typically folded structure. Debenzylation of (II) results in a dramatic flattening of the molecule structure giving th