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ChemInform Abstract: Preparation of Benzothieno(2,3-f)-1,4-oxazepin- and -thiazepin-5(2H)- ones and of Benzothieno(3,2-e)-1,4-diazepin-5-ones.

✍ Scribed by S. S. KHATANA; D. H. BOSCHELLI; J. B. KRAMER; D. T. CONNOR; H. BARTH; P. STOSS


Publisher
John Wiley and Sons
Year
2010
Weight
32 KB
Volume
28
Category
Article
ISSN
0931-7597

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Abstract

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A Facile Synthesis of Substituted 1,4-Be
✍ Wolfgang DΓΆlling; Matthias Biedermann; Helmut Hartung πŸ“‚ Article πŸ“… 1998 πŸ› John Wiley and Sons 🌐 English βš– 455 KB πŸ‘ 1 views

5(4H)-ones / 2-Chloro-N-cyanomethyl-N-methylnicotinamide / Aromatic nucleophilic substitution A new synthesis of pyrido[3,2-f][1,4]thiazepine derivatives 3 starting with 2-chloronicotinic acid (1), methylaminoacetonitrile hydrochloride and carbon disulfide is described. As proved by a crystal struct