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ChemInform Abstract: Phosphorylation of Amines by the UV-Light Mediated Fragmentation of a 2-Phosphabicyclo[2.2.2]octene 2-Oxide.

✍ Scribed by Gyoergy Keglevich; Helga Szelke; Zoltan Nagy; Andras Dobo; Tibor Novak; Laszlo Toke

Publisher: John Wiley and Sons
Year: 2010
Weight: 30 KB
Volume: 30
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.199952179

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Generation of methylenephosphine oxides

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## Differential thermal analysis and differential scanning calorimetry showed that the title compounds decomposed at 240-260°C with release of the fragment RP(0) = CH,. Mass spectral studies also showed this to be a fragmentation pathway. The extruded methylenephosphine oxide could be trapped with

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