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ChemInform Abstract: m-Chloroperbenzoic Acid Oxidation of 1,2-Dithietes: First Synthesis and Characterization of 1,2-Dithiete S-Oxides and Ethane-1,2-dithione S,S′-Dioxides (α-Disulfines).

✍ Scribed by J. NAKAYAMA; A. MIZUMURA; Y. YOKOMORI; A. KREBS; K. SCHUETZ

Book ID: 112028631
Publisher: John Wiley and Sons
Year: 2010
Weight: 33 KB
Volume: 27
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.199610168

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m-chloroperbenzoic acid oxidation of 1,2

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Reactions of acetylenes, possessing bulk

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The reaction of di-t-butylacetylene with S 2 Cl 2 , followed by purification with silica-gel column chromatography, gave 2,2,5,5-tetramethyl-4-oxo-3-hexanethione (4a) (37%) and 2,3-di-t-butylthiirene 1-oxide (5a) (10%), which were formed by hydrolysis of the initial product, 2,3-di-t-butyl-2,3-dichl

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