The reaction of di-t-butylacetylene with S 2 Cl 2 , followed by purification with silica-gel column chromatography, gave 2,2,5,5-tetramethyl-4-oxo-3-hexanethione (4a) (37%) and 2,3-di-t-butylthiirene 1-oxide (5a) (10%), which were formed by hydrolysis of the initial product, 2,3-di-t-butyl-2,3-dichl
✦ LIBER ✦
m-chloroperbenzoic acid oxidation of 1,2-dithietes: First synthesis and characterization of 1,2-dithiete s-oxides and ethane-1,2-dithione S,S′-Dioxides (α-Disulfines)
✍ Scribed by Juzo Nakayama; Ayako Mizumura; Yoshinobu Yokomori; Adolf Krebs; Karin Schütz
- Publisher
- Elsevier Science
- Year
- 1995
- Tongue
- French
- Weight
- 288 KB
- Volume
- 36
- Category
- Article
- ISSN
- 0040-4039
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