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ChemInform Abstract: Facile Total Synthesis of (.+-.)-Adalinine.

✍ Scribed by Naoki Yamazaki; Toshimasa Ito; Chihiro Kibayashi

Publisher: John Wiley and Sons
Year: 2010
Weight: 31 KB
Volume: 30
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.199920117

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✦ Synopsis

Facile Total Synthesis of (±)-Adalinine.

-Allylation of cyclic N-acyl-N,O-acetals using a combination of allylsilane and Lewis acid provides a useful construction of 6,6-disubstituted 2-piperidones. Compound (VIII) can be readily converted to the ladybird alkaloid (X) mentioned in the title. -(YAMAZAKI,

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