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ChemInform Abstract: Efficient Stereoselective Synthesis of the Epoxyacid Fragment of the Azinomycins.

✍ Scribed by R. S. COLEMAN; C. R. SARKO; J. P. GITTINGER

Publisher
John Wiley and Sons
Year
2010
Weight
30 KB
Volume
28
Category
Article
ISSN
0931-7597

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✦ Synopsis

Efficient Stereoselective Synthesis of the Epoxyacid Fragment of the Azinomycins.

-Sharpless asymmetric epoxidation/kinetic resolution of the racemic alcohol (III), effectively available by three different routes, proceeds with the opposite sense of enantioselection than predicted using literature precedent, providing the C17-C21-epoxyacid segment (X) of the azinomycins.

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