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ChemInform Abstract: Efficient and Versatile Synthesis of A-Ring Precursors of 1α,25- Dihydroxy-Vitamin D3 and Analogues. Application to the Synthesis of Lythgoe-Roche Phosphine Oxide.

✍ Scribed by A. MOURINO; M. TORNEIRO; C. VITALE; S. FERNANDEZ; J. PEREZ-SESTELO; S. ANNE; C. GREGORIO

Publisher
John Wiley and Sons
Year
2010
Weight
35 KB
Volume
28
Category
Article
ISSN
0931-7597

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✦ Synopsis

Efficient and Versatile Synthesis of A-Ring Precursors of 1α,25-Dihydroxy-Vitamin D3 and Analogues. Application to the Synthesis of Lythgoe-Roche Phosphine Oxide.

-Starting from 1-carvone (I) an efficient approach to the Lythgoe-Roche phosphine oxide (XII), an important vitamin D synthon, is reported. The procedure is based on the selective cleavage of epoxide (II) and its conversion to the esters (X). -(MOURINO,

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