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ChemInform Abstract: Alkylation Methodology for the Synthesis of 1,4-Disilacyclohexanes Using α,α′-Dilithiated Silanes.

✍ Scribed by M. SHIMIZU; M. IWAKUBO; Y. NISHIHARA; T. HIYAMA

Publisher
John Wiley and Sons
Year
2010
Weight
32 KB
Volume
29
Category
Article
ISSN
0931-7597

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New Methodology for the Synthesis of α,α-Dialkylamino Acids Using the "Self-Regeneration of Stereocenters" Method: α-Ethylα-phenylglycine. -Chiral oxazolidines such as (III) derived from phenylglycine are alkylated with ethyl iodide (IV) with high diastereoselectivity. Following hydrolytic deprotec